ASTM E755-1994(2003) 用液体色谱法作过氧化二异丙苯化验的测试方法

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【英文标准名称】:StandardTestMethodforDicumylPeroxide,Assay(LiquidChromatography)
【原文标准名称】:用液体色谱法作过氧化二异丙苯化验的测试方法
【标准号】:ASTME755-1994(2003)
【标准状态】:现行
【国别】:
【发布日期】:1994
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:E15.02
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:分析;药液;检定;液相色谱法;过氧化物
【英文主题词】:assay;dicumylperoxide;HPLC;liquidchromatography;peroxides
【摘要】:Thistestmethodprovidesameansfordeterminingthepercentofdicumylperoxideintechnicalandrefinedgradesofthismaterial.Thistestmethodisspecificfordicumylperoxide.Nointerferenceisencounteredfromdimethylbenzylalcohol,acetophenone,orotherminorimpuritiesnormallyassociatedwithcommercialdicumylperoxide.1.1Thistestmethodcoverstheassayofdicumylperoxideincommerciallyavailablerefinedgradesofdicumylperoxide.Technicalgradescanalsobeassayed,providedthatimpuritiesthatinterferechromatographicallyareabsent(seeNote1).Thesematerialsnominallycontainapproximately99and92%ofdicumylperoxide,respectively.Note18212;Intheassayoftechnicalgradedicumylperoxide,errorsarepossibleiftheproductcontainsanimpuritythateluteswiththesameretentiontimeastheinternalstandard.Achromatogramobtainedunderthetestconditionsminustheinternalstandardwilldeterminewhetheraninterferencesituationexistsintheassayofaparticulartechnicalgradeproduct.Ifanimpurityisnoted,anditsretentiontimeisslightlydifferentfromthatoftheinternalstandard,theinterferencecanoftenbeeliminatedbytheuseofacolumnknowntohaveahighplatecount.1.2Reviewthecurrentmaterialsafetydatasheets(MSDS)fordetailedinformationconcerningtoxicity,firstaidprocedures,andsafetyprecautions.1.3ThevaluesstatedinSIunitsaretoberegardedasthestandard.1.4Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.SpecificprecautionarystatementsaregiveninSection7.
【中国标准分类号】:G17
【国际标准分类号】:71_080_99
【页数】:4P.;A4
【正文语种】: